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Kinetica, Inc. offers a commercial sample
testing service for Differential Scanning Calorimetry (DSC). The technique of
DSC involves recording the energy necessary to establish a zero temperature
difference between a substance and a reference material against either time or
temperature as each specimen is subjected to an identical temperature program.
The ordinate value at any time or temperature is related to the difference in
heat flow between a standard sample and the unknown; this is related to the
kinetics of the process. Integration of the area under the heat flow curve
yields the enthalpy change associated with the thermal event of interest.
This service
provides a cost-effective method for obtaining kinetic and thermodynamic data
for condensed phase phenomena. Observable processes include simple phase
transitions, characterization of polymorphism, the kinetics and thermochemistry
for a variety of complex reactions.
Thermodynamic data for pure substances
include melting and boiling points, heat capacity, heat of fusion, heat of
solution, and heat of vaporization. Examples of complex processes include
oxidation of organic compounds, fuels and carbon combustion, polymerization and
resin curing reactions, explosives and pyrotechnic decomposition, and thermite
reactions. ASTM protocol is utilized whenever possible. Some of the applicable
procedures are listed in the table insert |